The Synthesis of Metalcarbon Nanocomposite Ni / C on the Basis of Polyacrylonitrile

Authors	L.V. Kozhitov¹ , D.G. Muratov¹^,² , E.V. Yakushko¹ , S.L. Kozhitov¹, A.G. Savchenko¹ , I.V. Shchetinin¹, S.G. Emelyanov³ , L.M. Chervjakov³
Affiliations	¹ National University of Science and Technology "MISIS", 4, Leninskii Pr., 119049 Moscow, Russia ² Institute of Petrochemical Synthesis named A.V. Topchiev of the Russian Academy of Sciences, 119991 Moscow, Russia ³ Southwest State University, 94, 50 Let Oktyabrya Str., 305040 Kursk, Russia
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Issue	Volume 5, Year 2013, Number 4
Dates	Received 05 August 2013; revised manuscript received 29 November 2013; published online 10 December 2013
Citation	L.V. Kozhitov, D.G. Muratov, E.V. Yakushko, et al., J. Nano- Electron. Phys. 5 No 4, 04007 (2013)
DOI
PACS Number(s)	61.48.De, 81. – b
Keywords	Metalcarbon nanocomposite (2) , Carbon matrix (2) , Nanoparticles of nickel.
Annotation	Metalcarbon nanocomposites based on polyacrylonitrile and nickel chloride are synthesized under the influence of infrared heat. The resulting materials represent a system of carbon matrix formed during the carbonization of PAN, and distributed in it nickel nanoparticles. The average size of the nanoparticles in the nanocomposite was 15-25 nm. It was found that the distribution of nickel nanoparticles sizes is determined by temperature synthesis nanocomposite. Thus with increasing temperature, the predominant average particle size of the metal increases, and the distribution is spread and shifted toward larger sizes.
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