Refinement Analysis using the Rietveld Method of Nd1.2Fe1O3 Oxide Material Synthesized by Solid-State Reaction

Автори E.H. Sujiono , A.C.M. Said, M.Y. Dahlan, R.A. Imran, S. Samnur
Приналежність

Laboratory of Materials Physics, Department of Physics, Universitas Negeri Makassar, Makassar, Indonesia

Е-mail e.h.sujiono@unm.ac.id
Випуск Том 10, Рік 2018, Номер 2
Дати Одержано 11.11.2017; у відредагованій формі 28.04.2018; опубліковано online 29.04.2018
Посилання E.H. Sujiono, A.C.M. Said, M.Y. Dahlan, et al., J. Nano- Electron. Phys. 10 No 2, 02034 (2018)
DOI https://doi.org/10.21272/jnep.10(2).02034
PACS Number(s) 61.05.cp, 74.62.Bf, 81.05.Bx,
Ключові слова Annealing time (2) , The Lattice constant, Solid-state reaction, The Rietveld method.
Анотація

Neodymium Ferrite Oxide (Nd1.2FeO3) has been successfully synthesized using solid state reaction by varying annealing time. Structural crystallographic characteristics were obtained by X-ray diffraction. The results of X-ray diffraction analysis showed the samples had been identified composed of NdFeO3 and Nd2O3 phase, with peak dominant correspond to hkl (121), FWHM value of 0.22° and estimated crystal size of 393 nm. Analysis using Rietveld methods obtained Nd1.2FeO3 oxide material has a crystal structure is orthorhombic with space-group of PNMA. The results is comparable as was reported elsewhere that the oxide material is useful for gas sensor application.

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