The Synthesis of Nanodispersed Magnetite Using Electrochemical Method

Authors S.Z. Kalaeva1 , N.S. Yamanina1, V.M. Makarov1 , I.N. Zaharova1, A.M. Shipilin2 , A.N. Solovyova1, M.E. Terzi2
Affiliations

1 Yaroslavl State Technical University, 88, Moskovskij prospect, 150023 Yaroslavl, Russia

2 Lomonosov Moscow State University, GSP-1, 1-2, Leninskiye Gory, 119991 Moscow, Russia

Е-mail [email protected]
Issue Volume 6, Year 2014, Number 3
Dates Received 19 May 2014; published online 15 July 2014
Citation S.Z. Kalaeva, N.S. Yamanina, V.M. Makarov, et al., J. Nano- Electron. Phys. 6 No 3, 03030 (2014)
DOI
PACS Number(s) 82.45.Aa. 82.80.Ej
Keywords Magnetite (6) , Electrochemical deposition (2) , Heated electrolyte, Powder XRD (2) , Magnetization (18) .
Annotation The purpose of the work was to obtain nanodispersed magnetite (Fe3O4) with fewer impurities comparing to its natural form. For this the electrochemical method of dissolution of steel sheets or shavings in the heated electrolyte was employed. In order to optimize the technological parameters of this process the structural and magnetic properties of the obtained materials were studied using powder X-ray diffraction and vibrational magnetometry techniques correspondingly.

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