Novel Synthesis and Structural Study of Cadmium Doped Cobalt Ferrite Nanoparticles through X-ray Diffraction Analysis
| Authors | Priyanka P. Kashid1,2, Shridhar N. Mathad1,2, , Rakesh M. Shedam1,2, Mahadev Shedam3 |
| Affiliations |
1Department of Engineering Physics, K.L.E. Institute of Technology, Gokul Road, Hubballi, 580027 Karnataka, India 2Visvesvaraya Technological University (VTU), 590018 Belagavi, India 3The New College, Kolhapur, India |
| Е-mail | physicssiddu@kleit.ac.in |
| Issue | Volume 16, Year 2024, Number 5 |
| Dates | Received 15 June 2024; revised manuscript received 22 October 2024; published online 30 October 2024 |
| Citation | Priyanka P. Kashid, Shridhar N. Mathad, [footnoteRef:], и др., J. Nano- Electron. Phys. 16 No 5, 05020 (2024) |
| DOI | https://doi.org/10.21272/jnep.16(5).05020 |
| PACS Number(s) | 68.37.Hk, 81.20.Ka |
| Keywords | Microstrain (ε), Crystallite size (D), X-ray density (Dx), Ferrite nanoparticles, Cd2+ substitution. |
| Annotation |
This paper investigated the structural properties of nano-crystalline Cd2+ doped cobalt ferrite (Co1 – xCdxFe2O4) nanoparticles were synthesized by co-precipitation method. X-ray diffraction study revealed the formation of mono phase cubic spinels. The crystallite size was found to be increased from 17 to 38 nm with increase of cadmium concentration. The other structural parameters like lattice constant (a), volume (V), hopping lengths (LA and LB), bond lengths (A-O and B-O), ionic radii (rA and rB), X-ray density (Dx), microstrain (ε) and dislocation density (D) were also estimated. Here, W-H and Size-Strain Plot methods were used for obtaining the values of lattice strain and crystallite size from the X-ray diffraction peak broadening analysis. Each method of analysis was different result because, the variation was found in calculated parameters. |
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List of References |
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