Synthesis and Characterization of Temperature Controlled SnO2 Nanoparticles by Solid-state Reaction Method
| Authors | Vijay Garg1, Harsh Sharma1, Divya Rehani2,3, Renu Kumari2,4, Vipin Kumar4, Manoj Kumar Tiwari5, Shailesh Narain Sharma3,6, Manish Saxena7 |
| Affiliations |
1Department of Physics, M.M. College Modinagar, 201204 Ghaziabad (U.P), India 2Dr. A.P.J. Abdul Kalam Technical University, 226031 Lucknow (U.P.), India 3Council of Scientific & Industrial Research-National Physical Laboratory, 110012 New Delhi, India 4Department of Physics, KIET Group of Institutions, 201206 Ghaziabad (U.P.), India 5Department of Electronics, Bhaskaracharya College of Applied Science, Delhi University, 110075 Delhi, India 6Academy of Scientific and Innovative Research ACSIR, 201002 Ghaziabad (U.P.), India 7Moradabad Institute of Technology, 244001 Moradabad, India
|
| Е-mail | drvgarg78@gmail.com |
| Issue | Volume 12, Year 2020, Number 4 |
| Dates | Received 14 April 2020; revised manuscript received 20 August 2020; published online 25 August 2020 |
| Citation | Vijay Garg, Harsh Sharma, Divya Rehani, et al., J. Nano- Electron. Phys. 12 No 4, 04004 (2020) |
| DOI | https://doi.org/10.21272/jnep.12(4).04004 |
| PACS Number(s) | 61.05.C, 61.82.Rx, 68.37.Hk, 82.20.Fw |
| Keywords | Tin oxide (8) , Nanoparticles (70) , Temperature (46) , Diffraction (21) , Tetragonal. |
| Annotation |
In the present work, nanoparticles of tin oxide (SnO2) annealed at temperatures of 400 °C, 500 °C, and 600 °C were prepared via solid-state reaction method. Structural and optical properties of prepared SnO2 nanoparticles were analyzed by X-ray diffractometer (XRD), scanning electron microscope (SEM), elemental study was performed by energy-dispersive X-ray spectroscopy (EDAX), Fourier transform infrared spectroscopy (FTIR), dynamic light scattering (DLS) and ultraviolet-visible (UV-Vis) absorption characterizing techniques. The X-ray diffraction pattern confirms the pure tetragonal rutile structure of tin oxide nanoparticles without any impurity phase. SEM images depict the formation of nanorods at all annealing temperatures of 400 °C, 500 °C, and 600 °C while EDAX analysis confirms the presence of Sn and O without any impurities. UV-Vis absorption spectra show that the band gap of prepared tin oxide nanoparticles decreases initially from 3.44 eV at 400 °C to 3.03 eV at 500 °C and further increases to 3.39 eV at 600 °C. FTIR spectrum confirms the presence of O–Sn–O bond along with one unwanted absorption peak. |
|
List of References |
Other articles from this number
1) Fabrication and Characterization of Polyaniline Nanofiber Films by Various Techniques [04001-1-04001-5]2) Nonlinear Model of Ice Surface Softening during Friction Taking into Account Spatial Heterogeneity of Temperature [04002-1-04002-6]
3) Effect of Different Heat Treatment Regimes on Electrical Properties and Microstructure of n-Si [04003-1-04003-5]
4) Simulation of Fracture Dynamics of Two-dimensional Titanium Carbide Ti2C under Different Types of Tensile Loading [04005-1-04005-4]
5) Features of Structural Organization of Nanodiamonds in the Polyethylene Glycol Matrix [04006-1-04006-6]
6) Characterization of Crystal Structure and Magnetic Properties of Zn(1 – x)MnxO (x = 0.086 and 0.090) Nanoparticles Synthesis Results Using Coprecipitation Method [04007-1-04007-4]
7) Effect of pH on Structural Morphology and Magnetic Properties of Ordered Phase of Cobalt Doped Lithium Ferrite Nanoparticles Synthesized by Sol-gel Auto-combustion Method [04008-1-04008-7]
8) A Low-profile Ultra-wideband LTCC Based Microstrip Antenna for Millimeter-wave Applications under 100 GHz [04009-1-04009-6]
9) Fabrication and Interpretation of Zinc-Cerium Composite: Structural and Thermal Studies [04010-1-04010-5]
10) Features of the Initial Stage of the Formation of Ti-Zr-Ni Quasicrystalline Thin Films [04011-1-04011-6]
11) Structural Studies of Mechanically Alloyed Fe1–xAlx Powder [04012-1-04012-5]
12) Hydrogen Adsorption on Li+ and Na+ Decorated Coronene and Corannulene: DFT, SAPT0, and IGM Study [04013-1-04013-6]
13) Realization of the Kelvin Probe System for the Surface Treatment of a Semiconductor [04014-1-04014-6]
14) Effect of Weak Confinement on the Optical Properties of Chemically Synthesized ZnS Nanoparticles [04015-1-04015-5]
15) Influence of the Vector Order Parameter on the Dynamics of 3D Ultrashort Pulses in Carbon Nanotubes [04016-1-04016-4]
16) Structural, Optical and Electrical Properties of Ce Doped SnO2 Nanoparticles Prepared by Surfactant Assisted Gel Combustion Method [04017-1-04017-6]
17) Sintering Temperature Dependent Structural and Mechanical Studies of BaxPb1 − xTiO3 Ferroelectrics [04018-1-04018-5]
18) Impact of Concentration of Nanoparticles on Characteristics of Transformer Oil [04019-1-04019-4]
19) Effect of the Porous Silicon Layer Structure on Gas Adsorption [04020-1-04020-5]
20) Light Emission from Silicon Structures with Dielectric Insulation [04021-1-04021-5]
21) Crystal Growth and Electro-optical Characterization of In2Se2.7Sb0.3 Compound [04022-1-04022-4]
22) Electron Energy in Rectangular and Cylindrical Quantum Wires [04023-1-04023-5]
23) An Ultra-low Power, High SNM, High Speed and High Temperature of 6T-SRAM Cell in 3C-SiC 130 nm CMOS Technology [04024-1-04024-4]
24) Measurement of the Angle of Attack of an Aerophysical Missile Complex in Flight Based on the Hall Effect Sensor and Electronic Measurement System [04025-1-04025-5]
25) Peculiarity of Elastic and Inelastic Properties of Radiation Cross-linked Hydrogels [04026-1-04026-5]
26) Structural and Optical Properties of Polycrystalline ZnO Nanopowder Synthesized by Direct Precipitation Technique [04027-1-04027-5]
27) Improving the Solar Collector Base Model for PVT System [04028-1-04028-5]
28) The Effect of Graphene Oxide on the Properties and Release of Drugs from Apatite-Polymer Composites [04029-1-04029-7]
29) Adhesion Strength of TiZrN/TiSiN Nanocomposite Coatings on a Steel Substrate with Transition Layer [04030-1-04030-6]
30) Thermal Effects on the Surface Morphology of an Ion-plasma Coating [04031-1-04031-5]
31) Some Properties and Structural Features of Poly(Vinyl Chloride)/Cu Films with Copper Nanoparticles Obtained by Exploding Wire Methodu [04032-1-04032-5]
32) Some Types of Carbon-based Nanomaterials as Contrast Agents for Photoacoustic Tomography [04033-1-04033-6]
33) Dynamics of Receiving Electroelastic Spherical Shell with a Filler [04034-1-04034-7]
34) The Effect of Chemical Composition and Electrolyte Temperature on the Size and Structure of Cadmium Sulfide Nanocrystals Obtained by the Electrolytic Method [04035-1-04035-6]
35) Morphological Features of the Nanoporous Structure in the Ammonium Nitrate Granules at the Final Drying Stage in Multistage Devices [04036-1-04036-6]
36) On Theory of Superheterodyne FELs with Longitudinal Electrostatic Undulator [04037-1-04037-5]
37) Experimental Investigation of the Distribution of Energy Deposited by FIB in Ion-beam Lithography [04038-1-04038-3]
38) Peculiarities of Magnetocaloric Effect in Ferromagnetic Cylindrical Nanowires with a Domain Wall [04039-1-04039-3]
