Synthesis and Characterization of Copper Indium Gallium Diselenide (CIGS) Nano-Crystalline Powder using SPEX Mill
| Автори | Priya S. Suryavanshi1, N.P. Kumar2, B.R. Rehani2, C.J. Panchal1 , S.G. Deshmukh3 |
| Приналежність |
1Applied Physics Department, Faculty of Technology and Engineering, The M. S. University of Baroda, 390001 Vadodara, Gujarat, India 2Centre for Chemical Sciences and Technology, Institute of Science and Technology, Jawaharlal Nehru Technological University, 500085 Hyderabad, Telangana, India 3SKN Sinhgad College of Engineering, Korti, 413304 Pandharpur, Maharashtra, India |
| Е-mail | cjpanchal_msu@yahoo.com |
| Випуск | Том 12, Рік 2020, Номер 2 |
| Дати | Received 15 February 2020; revised manuscript received 12 April 2020; published online 25 April 2020 |
| Посилання | Priya S. Suryavanshi, N.P. Kumar, B.R. Rehani, et al., J. Nano- Electron. Phys. 12 No 2, 02045 (2020) |
| DOI | https://doi.org/10.21272/jnep.12(2).02045 |
| PACS Number(s) | 61.43.Gt, 81.07.Wx |
| Ключові слова | CIGS (11) , Nanocrystalline powder, SPEX mill, EDAX (9) . |
| Анотація |
The CuIn1 – xGaxSe2 (CIGS) (x ( 0.3) nanocrystalline powder was synthesized by reacting to its constituent elements i.e. Copper, Indium, Gallium, and Selenium in a SPEX mill. The SPEX mill is a high-energy mill where the reaction between constituent elements takes place in solid-state to form a nanocrystalline compound powder. SPEX mill consists of tungsten lined hardened steel vials and tungsten carbide balls are used as grinding media. Three different size grinding media was used with ball to charge ratio of 10 : 1. The optimization of milling time was studied to obtain CIGS nanocrystalline powder using SPEX mill. The phase analysis by X-ray diffraction shows the formation chalcopyrite (tetragonal) structure of CIGS after 4 h of high-energy milling with an average crystallite size of 10-13 nm. Raman spectra peak at 174 cm – 1 confirms the formation of the CIGS phase. The compositional analysis by EDAX confirms the formation of the stoichiometric composition of CIGS. This study reveals that it is possible to synthesize CIGS nanocrystalline powder using SPEX mill. |
|
Перелік посилань |
Інші статті цього номера
1) Preface [02000-1-02000-1]2) Analytical Study of Graphene as a Novel Piezoresistive Material for MEMS Pressure Sensor Application [02001-1-02001-4]
3) Tunable Anti-Guiding Factor and Optical Gain of InGaAlAs/InP Nano-Heterostructure under Internal Strain [02002-1-02002-3]
4) Resistive Switching Property of Bmim(Br) Ionic Liquid under the Influence of ZnO Nanorods [02003-1-02003-4]
5) Morphology, Mechanical and Rheological Properties of Polylactic Acid Nanocomposite Film [02004-1-02004-4]
6) Synthesis and Photodetection Properties of Sonochemically Exfoliated Cu0.2Sn0.8Se Nanoparticles [02005-1-02005-5]
7) Structural Investigation and Optical Properties of Silver Nanoparticles Synthesis by Chemical Method [02006-1-02006-4]
8) Synthesis and Characterization of BSLT–NZFO Multiferroic Composite [02007-1-02007-3]
9) Effect of Conductive Filament Temperature on ZrO2 based Resistive Random Access Memory Devices [02008-1-02008-4]
10) Investigating the Effect of Sintering Treatment on Structural and Magnetic Properties of Fe3O4 Nanoparticles [02009-1-02009-4]
11) Deposition and Characterization of Indium Selenide Thin Films for Opto-electronic Devices [02010-1-02010-4]
12) Investigation of Supercapacitive Behaviour of Electrodeposited Cobalt Oxide Thin Film by Potentiostatic Mode [02011-1-02011-8]
13) Relation of Heat Transfer with the Growth Rate of InSb based Bulk Crystals Grown by VDS and its Effect on the Crystal Quality [02012-1-02012-5]
14) Study of Surface Morphology and Optical Properties of ZnO Thin Film Synthesized Using CBD Technique [02013-1-02013-3]
15) Correlation Between the Entropy Degree and Properties of Multi-component (High-entropy) Film Materials [02014-1-02014-3]
16) Determination of Thickness and Optical Parameters of Thin Films from Reflectivity Spectra Using Teaching-Learning Based Optimization Algorithm [02015-1-02015-6]
17) Study of Structural and Optical Properties of FeS2 Nanoparticles Prepared by Polyol Method [02016-1-02016-3]
18) Surfactant Free Synthesis and Study of Vanadium Pentoxide Nanostructure [02017-1-02017-3]
19) Temperature Variation of Debye-Waller Factor and Mean Square Displacement for bcc Metals Using Density Based Pseudopotential [02018-1-02018-3]
20) Theoretical Study of Structural and Dynamical Properties of Liquid Ag74Ge26 Alloys Using Pseudopotential Method [02019-1-02019-3]
21) The Comparative Study of Electrical Resistivity of bcc Liquid Transition Metals [02020-1-02020-3]
22) Theoretical Investigations of Lattice Dynamics and Dynamical Elastic Constants of Rh0.6Pd0.4 and Rh0.2Pd0.8 Binary Alloys Using Transition Metal Pseudopotential [02021-1-02021-3]
23) The Study of Lattice Dynamics and Dynamical Elastic Constants for Calcium (Ca) and Strontium (Sr) in bcc Phase Using Pseudopotential Approach [02022-1-02022-4]
24) Fabrication of Silica/PMMA Composite Based Superhydrophobic Coating by Drop Casting Method [02023-1-02023-4]
25) Tin Oxide Nanostructure Fabricated by Thermal Evaporation as Potential NO2 Sensor [02024-1-02024-3]
26) Bipolar Resistive Switching Characteristics of Ex-situ Synthesized TiO2-ZnO Nanocomposite [02025-1-02025-4]
27) Effect of Sm Doping on Structural and Dielectric Properties of CoFe2O4 Ferrite [02026-1-02026-3]
28) Sol-gel Synthesis and Supercapacitive Characterization of Bismuth Vanadate [02027-1-02027-4]
29) Structural Properties of (Ba0.97Ca0.03Ti0.985Sn0.015O3)-(K0.5Na0.5NbO3)Lead-free Electroceramics [02028-1-02028-4]
30) Resistive Switching Characteristics of Electrochemically Anodized Sub-stoichiometric Ti6O Phase [02029-1-02029-4]
31) Suppression of Optical Feedback in Laser Diodes Using Multilayered Broad-band Ultra-low Reflective Facets-coating [02030-1-02030-5]
32) Ground State Stability and Thermal Properties of ErCu Using First Principles Study [02031-1-02031-4]
33) Electrical Transport in Polyvalent Liquid Bismuth and Antimony Metals [02032-1-02032-5]
34) Quasiharmonic r–space Computational Scheme for Phonon Dynamics: Case Study of Calcium Oxide [02033-1-02033-4]
35) Shock Wave Treated PVA Films as Alternative Bio Degradable Polymer for Packaging Industry [02034-1-02034-4]
36) Resistive Switching Memory Properties of Electrodeposited Cu2O Thin Films [02035-1-02035-4]
37) Study of BaCl doped ZTS Crystals Grown by Gel Method [02036-1-02036-3]
38) Studies on DC Magnetron Sputtered AZO Thin Films for HIT Solar Cell Application [02037-1-02037-6]
39) Room Temperature Synthesized TiO2/Bi2Se3 Bilayer Thin Film by Simple Chemical Route: Study the Effect of Deposition Time of Bismuth Selenide on Physical Properties of Film [02038-1-02038-4]
40) Simple Thiophene Based Organic Dyes as Active Photosensitizers for DSSC Application: from Molecular Design to Structure Property Relationship [02039-1-02039-5]
41) Effect of Annealing on Magnetic and Structural Properties of FeNi Thin Films [02040-1-02040-4]
42) Aloe Vera Mediated Green Synthesis of ZnO Nanostructure under Sol-gel Method: Effect of Antimicrobial Activity [02041-1-02041-5]
43) Fabrication of Roughness Enhanced Hydrophobic Coatings [02042-1-02042-4]
44) Structural and Electrochemical Properties of Polymer Blend Based ZnO Nanocomposite Solid Polymer Electrolytes by Spin–Coating Method [02043-1-02043-5]
45) Instantaneous Fabrication of Thin MEMS Features by Copper Electrodeposition Using Modified Inkjet Printer [02044-1-02044-4]
